|
Chemistry 344
Fall 2004
Home
Instructors
Lab Safety Policies
Course Policies
Grading
Schedule of Experiments Lab/Discussion Sections
Prelab Reading Assignments
Spectroscopy Power Point Slides
Revised
Friedel-Crafts Experiment
| |
Read the section
on safety at the beginning of the lab manual. Anybody with sensitive medical
conditions should consult with the laboratory director before the start of the
course. If you are pregnant, especially in the first trimester, it is
strongly recommended that you do not enroll in this course at this time.
I. Dress Code:
|
A. Eye
protection: |
Eye
protection is required for any person in the laboratory. This is strictly
enforced! Students who have to be frequently reminded about eye protection
will receive poor grades for lab technique, and in extreme cases, they will
be dismissed from the course. The required protection for your eyes are
goggles. Plastic visitor's glasses are not acceptable because they are
easily damaged by the solvents in the laboratory and don’t provide adequate
protection against splashes. If you have any questions regarding the
requirement for proper eye protection equipment, see the Director of the
Organic Labs on the first day of the course. |
|
|
|
|
B. Attire: |
You must wear
footwear that fully covers your feet. No sandals! No open toe shoes.
Since chemicals can damage clothes, it is best to wear clothes that you
wouldn’t mind disposing of in case they are damaged. We strongly recommend
that you wear a shirt that covers the entire torso with no exposed skin at
the waist. Shorts are allowed in the lab. |
II. Chemical Handling
in Lab:
|
A.
Chemical Hazards |
Read through
the lab safety section of each chapter. Know the chemical toxicity of each
compound that you are using and working with. |
|
|
|
|
B.
Wearing gloves: |
It’s
recommended that you were gloves at any time there is a likelihood of
chemicals directly contacting your hands. Disposable gloves are provided
free of charge. You should use them as often you as you need them. |
|
|
|
|
C. Gloves
outside the laboratory: |
Anytime you
need to go outside of the laboratory (e.g. restroom, instrument room,
stockroom) you need to remove your gloves. This is for the safety and
protection of everyone. Do not under any circumstances touch any doorknobs,
door handles, computer keyboards or mouse, while you are wearing gloves.
|
|
|
|
D. Waste disposal
|
Make sure you
properly dispose of the chemicals when you’re done with the experiment.
Solid organic waste will go into labeled waste containers; solvents will go
into one of the organic carboys. All salts and aqueous solutions can go
down the drain. If you are not clear on proper handling of a chemical, ask
your TA. |
III. Safe Practices in
the Laboratory:
|
A.
Health: |
When you’re
working in lab, if you feel dizzy or lightheaded, you should notify your TA
right away. If you are unable to get to your TA, have a coworker get your
TA. |
|
|
|
|
B. Cuts: |
If you cut
yourself, notify your TA, remove any foreign matter (e.g. broken glass) from
the cut, and rinse the cut thoroughly with water. Apply direct pressure
over the wound to stop the bleeding |
|
|
|
|
C. Spills
on skin: |
Spills on the
skin can usually be avoided by being neat and organized and careful.
Anytime you have a spill on your skin, you should wash the area of the skin
with a lot of water. Make sure you also consult your TA. |
|
|
|
|
D. Broken
thermometers: |
Most
laboratory thermometers contain mercury. If you break your thermometer, you
need to carefully clean up any spilled mercury according to stardard
procedures and properly dispose of the broken thermometer and mercury.
Notify your TA and he/she will help clean up the mercury spill. |
|
|
|
|
E. Heating baths: |
Be extremely
careful when you are handling steam and sand heating baths. They can get
very hot and represent a skin burn hazard. |
|