| Reference: | Huang, A.; Kodanko, J. J.; Overman, L. E. J. Am. Chem. Soc. 2004, 126, 14043. DOI |
| Keywords: | Ketal -> Diol • Diol-1,2 cleavage • Aryl-OMe -> Aryl-OH • Aryl-OH -> Aryl-OC(O)NR2 • Lactam enolate+Alkyl-X • Reductive amination, Al-H • Amine-5 • N-H -> N-Alkyl • |
| Reagents: | KN(SiMe3)2 • DMPU (solvent) • TsOH • Periodate, sodium • NH2Me • AlH4-Li+ • BBr3 • NaH • Isocyanate • |