| Reference: | Aungst, R. A.; Chan, C.; Funk, R. L. Org. Lett. 2001, 3, 2611. DOI |
| Keywords: | O-H -> O-SO2R • Li/Br -> Li-Vinyl • Ketone-1,3-di enolate+Alkyl-X • Hydrogenolysis N-O • Alkyl-OH -> Alkyl-I(2°) • Dehydrohalogenation -> Ene • Dehydration -> Enone • Li-Vinyl+Ketone • Nitrile oxide Cycloaddition • Oxime -> Nitrile oxide • |
| Reagents: | POBr3 • DMF (react) • NH2OH • Vinyl-Li • Ethylene dibromide • AlH(OtBu)3-Li+ • PPh3, I2 • DBU • BuLi(tert) • H2, RaNi • MeSO2Cl, NEt3 • DBU • Vilsmeier reagent • Imidazole • TsNClNa • |