| Reference: | Huckins, J. R.; Vicente, J. de; Rychnovsky, S. D. Org. Lett. 2007, 9, 4757. DOI |
| Keywords: | O-SiMe2tBu -> O-H --- Alkyl-OH -> Aldehyde --- O-H -> O-C(O)R --- O-H -> O-SiMe2tBu --- CarboxAcid -> CarboxAmide(Weinreb) --- Nozaki-Hiyama coupling --- Cr-Vinyl+Aldehyde --- Claisen-Ireland --- Li/S -> Li-Alkyl --- CarboxAmide(Weinreb)+Li-Alkyl |
| Reagents: | BuLi(n) --- LiDBB --- Fluoride, Bu4N+ --- Dess-Martin --- Propenyl-Br --- CrCl2 --- DMAP --- SiMe2tBu-OTf --- AcOH --- NMe(OMe)-H --- Carbodiimide |