Structure Determination Using NMR

Chem 605 - H. J. Reich

Course Notes
  General
    Syllabus
    NMR Bibliography
  Proton NMR (HMR)
    5.00 - NMR experiment, PDF 0-2
    5.01 - Integration
    5.02 - Chemical Shifts (δ)
    5.03 - Coupling (J), PDF 3-6
    5.04 - Geminal J
    5.05 - Vicinal J
    5.06 - Long-range J
    5.07 - Spin nomenclature, PDF 7-16
    5.08 - NMR symmetry
    5.09 - Second order
    5.10 - AX and AB
    5.11 - AX2 and AB2
    5.12 - ABX,
    5.13 - ABX3
    5.14 - A2B2
    5.15 - AA'BB'
    5.16 - Virtual coupling
  H-NMR Data (HDATA)
    9.1 - Proton shifts
    9.4 - NMR solvents
    9.5 - Shift calculations sp3
    9.6 - Shift calculations sp2
    9.7 - J(H-H) data


    9.8 - Spectra Gallery New: 2017-02
  Carbon NMR (CMR)
    6.1 - Spectra,
    6.2 - Chemical Shifts
    6.3 - sp3 Carbons
    6.4 - sp2 Carbons
    6.5 - One-bond J(CH)
    6.6 - Two, three-bond J(CH)
    6.7 - Long-range J(CH)
    6.8 - Assignment
  Carbon Data (CDATA)
    10.4 - C-13 Shift data
    10.5 - J(C-H) data
    10.6 - J(C-C) data
  Multinuclear NMR
    7.1 - Nuclear properties
    7.2 - Effects on H, C NMR
    7.3 - Spin 1/2 Nuclei
    7.4 - Quadrupolar nuclei
    11.1 - NMR Nuclei:
       Main group
       Transition metals
       Actinides
    11.2 - Shift and J data
        F-19, P-31, Se-77, B-11
  Topics in NMR
    8.1 - Relaxation
    8.2 - NOE
    8.3 - DNMR,
    8.4 - Saturation Transf.,
    8.5 - Saunders Isotope,
    8.7 - Shift reagents
    8.9 - Multipulse NMR - 2D

Exams, Problems
   Practice Exam 1, Answer
   Another Exam 1, Answer
   Practice Exam 2, Answer
   Another Exam 2, Answer
   Exam 2 Answer
   Practice Exam 3, Answer
   Another Exam 3, Answer

NMR Data
   NMR Solvents
   NMR Acronyms
   NMR Periodic Table

NMR Simulation
   WINDNMR

Spectra Excercises
   James Nowick, UC Irvine
   Craig Merlic, UCLA
   Bradley Smith, Notre Dame


H. J. Reich home page
Organic Chem Info
Total Syntheses
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